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分析機器 Gamry Reference 3000のPDF クイック・スタート・マニュアルをオンラインで閲覧またはダウンロードできます。Gamry Reference 3000 16 ページ。 Usb potentiostat installation
Gamry Reference 3000 にも: クイック・スタート・マニュアル (4 ページ)
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Reference 3000
Potentiostat/Galvanostat/ZRA Quick-Start Guide
virtual LED
Tip: If the selected potentiostat has never been calibrated, no
Current Calibration Status information is displayed in the bottom
half of the Potentiostat Calibration window. The calibration
information in a Reference 3000 is stored inside the unit and moves
with the unit from computer to computer.
However, if the potentiostat has already been calibrated this window
displays information about the most recent calibration.
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To confirm hardware recognition:
1)
2)
3)
4)
Calibration Preparation
Before you can use a new potentiostat, you must calibrate it
using the Universal Dummy Cell 4 shipped with the
potentiostat.
Recalibrate a potentiostat every six months or after moving
the potentiostat to a different environment.
To prepare for calibration:
1)
2)
3)
Start Calibration Utility and Select the
Potentiostat
If you see a green virtual LED and the name of the
potentiostat installed in the PC, you are ready to calibrate.
A Utilities submenu in the Experiment menu is always
available in Framework. The Utilities submenu always
includes the Calibrate Instrument choice.
The other submenus available from the Experiment menu
depend on the selections you made when installing the
Gamry software. An Experiment submenu is available for
every Gamry software package you installed, although you
can run experiments only for authorized software packages.
To start the calibration utility:
1)
2)
3)
4)
Gamry Instruments, Inc. © 2008
Look at the top left corner of Framework screen (below
the menu bar). When the Framework window first opens
"Initializing Devices" is displayed.
After the potentiostat has been initialized, the "Devices
Present" line should display the name (label) assigned to
the potentiostat. A green "virtual LED" should also be
displayed to symbolize that the potentiostat is ready for
use.
When a potentiostat is in use, the virtual LED turns
yellow. The virtual LED and potentiostat label should
always be displayed.
If the name of the potentiostat is displayed and the
virtual LED is green, you are ready to calibrate the
potentiostat as described in the next subsection.
However, if a potentiostat's name is not displayed, the
Reference 3000 may not be installed correctly. Check
the power connections and USB cable. Make sure the
USB connector on the computer is enabled or
connected. Verify the Power and USB LED's on the
instrument are lit.
Let the Reference 3000 warm up for at least 30 minutes.
Place the dummy cell inside the Calibration Shield.
Make sure the cell cable supplied with the potentiostat is
firmly connected to the potentiostat to be calibrated.
Open the Potentiostat Calibration window by selecting
Experiment > Utilities > Calibrate Instrument from the
Framework menu bar.
In the Potentiostat Calibration window select the option
button labeled with the name of the potentiostat to be
calibrated.
Select the calibration type "Both".
Click on OK. The Potentiostat Calibration window
remains open. The Connection Information window will
open. It contains general instructions for using the
Universal Dummy Cell (UDC). Specific instructions for
using the Universal Dummy Cell are in this document
(see below).
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